Syntheses and Crystal Structures of Benzyltin（Ⅳ） Derivatives of 2-Mercaptobenzothiazole-中国Betway体育网页登陆

摘要 Thecomplexes(PhCH2)2Sn(MBT)2(2)and(PhCH2)3Sn(MBT)(3)(HMBT:2-mercaptobenzothiazole)havebeensynthesizedandcharacterizedbyelementalanalyses,andIR,^1H,^13C,^119SnN-MRspectrometriesandX-raydiffraction.Studiesonthecrystalstructuresof2and3showthatHMBTactsasbidentateligandthroughchelationofNandSatoms.Complex2containsasix-coordinatetinatomwiththeaxialangleC(15)-Sn(1)-C(22)129.6(2)°.Andthetinenvironmentofcomplex3isadistortedcis-trigonalbipyramidwithC(8)-Sn(1)-N(1)158.80°.

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Syntheses and Crystal Structures of Benzyltin（Ⅳ） Derivatives of 2-Mercaptobenzothiazole

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Syntheses and Crystal Structures of Benzyltin（Ⅳ） Derivatives of 2-Mercaptobenzothiazole

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